
11
9. Open up the nitrogen line. Make sure the leftmost flowmeter by the DSC is reading
between 10 and 50 mL.
10. Before opening the liquid nitrogen dewar, check the level. If it is empty, ask someone in
charge of the instrument for help in how to fill it up. If it is sufficiently full, turn it on
11. Click Start at the bottom right hand of the window. This will open the experiment on the
module. A prompt wil appear in the green bar that says Going to Insert Temperature.
Click OK. A prompt will appear in the green bar that says Waiting for sample insertion.
Click OK. The bar will go red.
12. When the sample is done running, remove the sample and click OK. DSC samples can be
stored and used for multiple runs. Turn off the liquid nitrogen and nitrogen.
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